A rapid, specific, and sensitive method for the simultaneous quantitation of organophosphates (fenitrothion (MEP), malathion, and phenthoate (PAP)), glufosinate (GLUF), and glyphosate (GLYP) in human serum and urine by gas chromatography-mass spectrometry (GC-MS) has been validated. All of the targeted compounds together with the internal standard were extracted from the serum and urine using a mix-mode TiO-C(18) monolithic spin column. The recovery of organophosphates from serum and urine ranged from 12.7 to 49.5
作者:Takeshi, Saito;Hiromichi, Aoki;Akira, Namera;Hiroshi, Oikawa;Shota, Miyazaki;Akihiro, Nakamoto;Sadaki, Inokuchi
来源:Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 2011 年 27卷 10期